<?xml version="1.0" encoding="UTF-8"?><eml:eml xmlns:eml="https://eml.ecoinformatics.org/eml-2.2.0" xmlns:stmml="http://www.xml-cml.org/schema/stmml-1.1" xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance" xsi:schemaLocation="https://eml.ecoinformatics.org/eml-2.2.0 https://lter.kbs.msu.edu/docs/eml-2.2.0/eml.xsd" packageId="knb-lter-kbs.119.24" system="KBS LTER"><access scope="document" order="allowFirst" authSystem="knb"><allow><principal>uid=KBS,o=lter,dc=ecoinformatics,dc=org</principal><permission>all</permission></allow><allow><principal>uid=sbohm,o=lter,dc=ecoinformatics,dc=org</principal><permission>all</permission></allow><allow><principal>public</principal><permission>read</permission></allow></access><dataset><alternateIdentifier system="lter.kbs.msu.edu">https://lter.kbs.msu.edu/datasets/119.eml</alternateIdentifier><title>GLBRC Deep Core Soil Surveys at the Kellogg Biological Station, Hickory Corners, MI  (2008 to 2017)</title><creator><individualName><givenName>G.</givenName><surName>Robertson</surName></individualName><organizationName>Michigan State University</organizationName><address><deliveryPoint>3700 East Gull Lake Drive</deliveryPoint><city>Hickory Corners</city><administrativeArea>MI</administrativeArea><postalCode>49060</postalCode><country>US</country></address><phone phonetype="phone">(269) 760-8364</phone><phone phonetype="fax">(269)671-2351</phone><electronicMailAddress>robert30@msu.edu</electronicMailAddress><userId directory="http://orcid.org">0000-0001-9771-9895</userId></creator><pubDate>2026-04-10</pubDate><abstract><section><title>Dataset Abstract</title><para></para><para>original data source http://lter.kbs.msu.edu/datasets/119</para></section></abstract><keywordSet><keyword keywordType="place">LTER</keyword><keyword keywordType="place">KBS</keyword><keyword keywordType="place">Kellogg Biological Station</keyword><keyword keywordType="place">Hickory Corners</keyword><keyword keywordType="place">Michigan</keyword><keyword keywordType="place">Great Lakes</keyword></keywordSet><keywordSet><keyword keywordType="theme">organic</keyword><keyword keywordType="theme">matter</keyword><keyword keywordType="theme">phosphorus</keyword><keyword keywordType="theme">magnesium</keyword><keyword keywordType="theme">P</keyword><keyword keywordType="theme">OM</keyword><keyword keywordType="theme">soil</keyword><keyword keywordType="theme">potassium</keyword><keyword keywordType="theme">chemistry</keyword><keyword keywordType="theme">pH</keyword><keyword keywordType="theme">cation</keyword><keyword keywordType="theme">exchange</keyword><keyword keywordType="theme">capacity</keyword></keywordSet><keywordSet><keyword>Inorganic Nutrients</keyword><keyword>Disturbance</keyword><keyword>Organic Matter</keyword><keywordThesaurus>LTER Core Research Area</keywordThesaurus></keywordSet><keywordSet><keyword keywordType="theme">farming</keyword><keyword keywordType="theme">biota</keyword><keywordThesaurus>https://apps.usgs.gov/thesaurus/thesaurus-full.php?thcode=15</keywordThesaurus></keywordSet><intellectualRights><para>Data in the KBS LTER core database may not be published without written permission of the lead investigator or project director. These restrictions are intended mainly to preserve the primary investigators' rights to first publication and to ensure that data users are aware of the limitations that may be associated with any specific data set. These restrictions apply to both the baseline data set and to the data sets associated with specific LTER-supported subprojects.</para><para>All publications of KBS data and images must acknowledge KBS LTER support.</para></intellectualRights><coverage><geographicCoverage><geographicDescription>The areas around the Kellogg Biological Station in southwest Michigan</geographicDescription><boundingCoordinates><westBoundingCoordinate>-85.404699</westBoundingCoordinate><eastBoundingCoordinate>-85.366857</eastBoundingCoordinate><northBoundingCoordinate>42.420265</northBoundingCoordinate><southBoundingCoordinate>42.391019</southBoundingCoordinate></boundingCoordinates></geographicCoverage><temporalCoverage><rangeOfDates><beginDate><calendarDate>2008-01-01</calendarDate></beginDate><endDate><calendarDate>2017-12-07</calendarDate></endDate></rangeOfDates></temporalCoverage></coverage><contact><organizationName>Kellogg Biological Station</organizationName><positionName>Data Manager</positionName><electronicMailAddress>lter.data.manager@kbs.msu.edu</electronicMailAddress><onlineUrl>http://lter.kbs.msu.edu</onlineUrl><userId directory="https://ror.org/">02vkce854</userId></contact><publisher><organizationName>KBS LTER</organizationName></publisher><methods><methodStep><description>Soils of the GLBRC Biofuel Cropping System Experiment (BSCE) and Scale-Up Experiment are sampled to measure and monitor a variety of physical and chemical factors, including soil bulk density, texture, pH, moisture, organic carbon, inorganic nitrogen, and several other nutrients. Both surface and deep-core soil samples are collected. Currently surface samples to 25 cm are collected in annual crop treatments on an annual basis and analyzed for inorganic nitrogen and for fertilizer recommendations and collected in perennial crop treatments every three years. Deep-core sampling to 1 meter occurs every 5 to 10 years to primarily examine long-term changes in organic carbon and nitrogen.</description><protocol id="protocol_158"><title>Soil Sampling of BCSE and Scale-Up Experiment</title><creator><positionName>Data Manager</positionName></creator><distribution><online><url>http://lter.kbs.msu.edu/protocols/158</url></online></distribution></protocol></methodStep><methodStep><description>Soil total carbon and nitrogen as well as the ratio of C:N are important attributes of soil fertility. Both total C and N are measured by a combustion method that does not differentiate between organic and inorganic forms of the elements. In most soils, inorganic N is a tiny fraction of total N so total N is synonymous with organic N. Inorganic C, on the other hand, can be a significant portion of total C in soils with carbonate minerals. Extensive testing of KBS surface soils has shown soil inorganic C to be non-detectable; thus total C in KBS surface soils is synonymous with total organic carbon (TOC).
However, carbonates may still be present in deep or recently limed soils, which must be tested for inorganic carbon and, if present, the carbonates removed via acid fumigation (described below) prior to total C analysis. Inorganic C can also be analyzed separately via the inorganic C protocol.
To measure total C and N, subsamples of dried, finely ground soil are weighed into small foil capsules that are combusted in an automated CHN analyzer that measures the amount of released CO2 and N2 by gas chromatography. Final values are expressed as the percentage of carbon or nitrogen in dry soil. If inorganic C has been confirmed to be absent, removed, or analyzed separately and subtracted, values can be expressed as total organic C.
Sampling frequency depends on experiment and research objectives. Since 2001, soils of the LTER Main Cropping System Experiment are analyzed for total C and N as part of the decadal deep soil core (whole profile) sampling program, usually in late fall of wheat years.</description><protocol id="protocol_37"><title>Soil Total Carbon and Nitrogen</title><creator><positionName>Data Manager</positionName></creator><distribution><online><url>http://lter.kbs.msu.edu/protocols/37</url></online></distribution></protocol></methodStep><methodStep><description>The Costech Elemental Combustion System 4010 is an automated combustion analyzer used to determine total carbon and nitrogen in soil and plant samples. This system employees a helium carrier gas to bring combustion gases to a gas chromatographic separation column and thermal conductivity detector. More information about the analyzer can be obtained from Costech Analytical Technologies (26074 Avenue Hall, Suite 13, Valencia, CA 91355 – USA or http://www.costechanalytical.com/)
For preparation and analysis of plant material, see https://lter.kbs.msu.edu/protocols/40. For preparation and analysis of soil, see https://lter.kbs.msu.edu/protocols/37.</description><protocol id="protocol_148"><title>Costech Elemental Combustion System CHNS-O (ECS 4010)</title><creator><positionName>Data Manager</positionName></creator><distribution><online><url>http://lter.kbs.msu.edu/protocols/148</url></online></distribution></protocol></methodStep></methods><dataTable><alternateIdentifier system="lter.kbs.msu.edu">https://lter.kbs.msu.edu/datatables/364</alternateIdentifier><entityName>Kellogg Biological Station LTER: Soil Chemistry from Deep Cores (KBS093-002)</entityName><entityDescription>Deep core soil samples analyzed for pH, lime index, phosphorus, potassium, calcium, magnesium, cation exchange capacity and organic matter.
KBS samples are analyzed by the Michigan State University Soil and Plant Nutrient Laboratory .</entityDescription><physical><objectName>Soil+Chemistry+from+Dep+Cores.csv</objectName><encodingMethod>None</encodingMethod><dataFormat><textFormat><numHeaderLines>34</numHeaderLines><numFooterLines>1</numFooterLines><recordDelimiter>\n</recordDelimiter><attributeOrientation>column</attributeOrientation><simpleDelimited><fieldDelimiter>,</fieldDelimiter><collapseDelimiters>no</collapseDelimiters><quoteCharacter>"</quoteCharacter><literalCharacter>\</literalCharacter></simpleDelimited></textFormat></dataFormat><distribution><online><url>https://lter.kbs.msu.edu/datatables/364.csv</url></online></distribution></physical><attributeList><attribute><attributeName>sample_date</attributeName><attributeDefinition>date the soil core was collected</attributeDefinition><measurementScale><dateTime><formatString>YYYY-MM-DD</formatString><dateTimePrecision>1</dateTimePrecision><dateTimeDomain><bounds><minimum exclusive="true">1987-4-18</minimum></bounds></dateTimeDomain></dateTime></measurementScale></attribute><attribute><attributeName>treatment</attributeName><attributeDefinition>experimental treatment</attributeDefinition><measurementScale><nominal><nonNumericDomain><textDomain><definition>experimental treatment</definition></textDomain></nonNumericDomain></nominal></measurementScale></attribute><attribute><attributeName>replicate</attributeName><attributeDefinition>replicate nested within treatment</attributeDefinition><measurementScale><nominal><nonNumericDomain><textDomain><definition>replicate nested within treatment</definition></textDomain></nonNumericDomain></nominal></measurementScale></attribute><attribute><attributeName>main_or_microplot</attributeName><attributeDefinition>whether the main or the microplot was sampled</attributeDefinition><measurementScale><nominal><nonNumericDomain><textDomain><definition>whether the main or the microplot was sampled</definition></textDomain></nonNumericDomain></nominal></measurementScale></attribute><attribute><attributeName>campaign</attributeName><attributeDefinition>type of soil sampling</attributeDefinition><measurementScale><nominal><nonNumericDomain><textDomain><definition>type of soil sampling</definition></textDomain></nonNumericDomain></nominal></measurementScale></attribute><attribute><attributeName>top_depth</attributeName><attributeDefinition>upper soil sampling depth</attributeDefinition><measurementScale><interval><unit><standardUnit>centimeter</standardUnit></unit><numericDomain><numberType>integer</numberType></numericDomain></interval></measurementScale></attribute><attribute><attributeName>bottom_depth</attributeName><attributeDefinition>lower soil sampling depth</attributeDefinition><measurementScale><interval><unit><standardUnit>centimeter</standardUnit></unit><numericDomain><numberType>integer</numberType></numericDomain></interval></measurementScale></attribute><attribute><attributeName>ph</attributeName><attributeDefinition>pH of soil solution</attributeDefinition><measurementScale><interval><unit><standardUnit>dimensionless</standardUnit></unit><numericDomain><numberType>real</numberType></numericDomain></interval></measurementScale></attribute><attribute><attributeName>lime_index</attributeName><attributeDefinition>indicator of potential acidity</attributeDefinition><measurementScale><interval><unit><customUnit/></unit><numericDomain><numberType>real</numberType></numericDomain></interval></measurementScale></attribute><attribute><attributeName>p_ppm</attributeName><attributeDefinition>phosphorus concentration</attributeDefinition><measurementScale><ratio><unit><customUnit>milligramsPerKilogram</customUnit></unit><numericDomain><numberType>real</numberType></numericDomain></ratio></measurementScale></attribute><attribute><attributeName>k_ppm</attributeName><attributeDefinition>potassium concentration</attributeDefinition><measurementScale><ratio><unit><customUnit>milligramsPerKilogram</customUnit></unit><numericDomain><numberType>real</numberType></numericDomain></ratio></measurementScale></attribute><attribute><attributeName>ca_ppm</attributeName><attributeDefinition>calcium concentration</attributeDefinition><measurementScale><ratio><unit><customUnit>milligramsPerKilogram</customUnit></unit><numericDomain><numberType>real</numberType></numericDomain></ratio></measurementScale></attribute><attribute><attributeName>mg_ppm</attributeName><attributeDefinition>magnesium concentration</attributeDefinition><measurementScale><ratio><unit><customUnit>milligramsPerKilogram</customUnit></unit><numericDomain><numberType>real</numberType></numericDomain></ratio></measurementScale></attribute><attribute><attributeName>est_cec</attributeName><attributeDefinition>cation exchange capacity in meq/100g soil</attributeDefinition><measurementScale><ratio><unit><customUnit>milliEquivalentsPerHundredGram</customUnit></unit><numericDomain><numberType>real</numberType></numericDomain></ratio></measurementScale></attribute><attribute><attributeName>om_percent</attributeName><attributeDefinition>organic matter percent</attributeDefinition><measurementScale><ratio><unit><customUnit>gramsPerHectogram</customUnit></unit><numericDomain><numberType>real</numberType></numericDomain></ratio></measurementScale></attribute></attributeList></dataTable><dataTable><alternateIdentifier system="lter.kbs.msu.edu">https://lter.kbs.msu.edu/datatables/396</alternateIdentifier><entityName>Kellogg Biological Station LTER: Soil Horizons- Deep Core samples (KBS093_005)</entityName><entityDescription>Soil horizons of the GLBRC BCSE (Biofuel Cropping System Experiment) site. Soil core was collected with the deep core sampler.</entityDescription><physical><objectName>Soil+Horizons-+Dep+Core+samples.csv</objectName><encodingMethod>None</encodingMethod><dataFormat><textFormat><numHeaderLines>27</numHeaderLines><numFooterLines>1</numFooterLines><recordDelimiter>\n</recordDelimiter><attributeOrientation>column</attributeOrientation><simpleDelimited><fieldDelimiter>,</fieldDelimiter><collapseDelimiters>no</collapseDelimiters><quoteCharacter>"</quoteCharacter><literalCharacter>\</literalCharacter></simpleDelimited></textFormat></dataFormat><distribution><online><url>https://lter.kbs.msu.edu/datatables/396.csv</url></online></distribution></physical><attributeList><attribute><attributeName>sample_date</attributeName><attributeDefinition>sampling date</attributeDefinition><measurementScale><dateTime><formatString>YYYY-MM-DD</formatString><dateTimePrecision>1</dateTimePrecision><dateTimeDomain><bounds><minimum exclusive="true">1987-4-18</minimum></bounds></dateTimeDomain></dateTime></measurementScale></attribute><attribute><attributeName>treatment</attributeName><attributeDefinition>experimental treatment</attributeDefinition><measurementScale><nominal><nonNumericDomain><textDomain><definition>experimental treatment</definition></textDomain></nonNumericDomain></nominal></measurementScale></attribute><attribute><attributeName>replicate</attributeName><attributeDefinition>replicate nested within treatment</attributeDefinition><measurementScale><nominal><nonNumericDomain><textDomain><definition>replicate nested within treatment</definition></textDomain></nonNumericDomain></nominal></measurementScale></attribute><attribute><attributeName>station</attributeName><attributeDefinition>sampling station</attributeDefinition><measurementScale><nominal><nonNumericDomain><textDomain><definition>sampling station</definition></textDomain></nonNumericDomain></nominal></measurementScale></attribute><attribute><attributeName>top_depth</attributeName><attributeDefinition>top depth of soil sample</attributeDefinition><measurementScale><ratio><unit><standardUnit>centimeter</standardUnit></unit><numericDomain><numberType>real</numberType></numericDomain></ratio></measurementScale></attribute><attribute><attributeName>bottom_depth</attributeName><attributeDefinition>bottom depth of soil sample</attributeDefinition><measurementScale><ratio><unit><standardUnit>centimeter</standardUnit></unit><numericDomain><numberType>real</numberType></numericDomain></ratio></measurementScale></attribute><attribute><attributeName>horizon</attributeName><attributeDefinition>soil horizon name</attributeDefinition><measurementScale><nominal><nonNumericDomain><textDomain><definition>soil horizon name</definition></textDomain></nonNumericDomain></nominal></measurementScale></attribute><attribute><attributeName>comments</attributeName><attributeDefinition>notes specific to data row</attributeDefinition><measurementScale><nominal><nonNumericDomain><textDomain><definition>notes specific to data row</definition></textDomain></nonNumericDomain></nominal></measurementScale></attribute></attributeList></dataTable></dataset><additionalMetadata><metadata><stmml:unitList xmlns:stmml="http://www.xml-cml.org/schema/stmml-1.1" xmlns="http://www.xml-cml.org/schema/stmml" xsi:schemaLocation="http://www.xml-cml.org/schema/stmml-1.1 http://nis.lternet.edu/schemas/EML/eml-2.1.0/stmml.xsd"><stmml:unit id="milligramsPerKilogram" name="milligramsPerKilogram"/><stmml:unit id="milliEquivalentsPerHundredGram" name="milliEquivalentsPerHundredGram"/><stmml:unit id="gramsPerHectogram" name="gramsPerHectogram"/></stmml:unitList></metadata></additionalMetadata></eml:eml>